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ICS 13.060 Z16 DB46 DB 46/T 4822019/2019-11-20 2020-01-01 DB46/T 4822019 I.II 1.1 2.1 3.1 4.1 5.2 6.2 7.2 8.4 9.5 10.6 11.6 DB46/T 4822019 II GB/T 1.1-2009 2019 11 20 2020 DB46/T 4822019 1 1 5.0 ml 0.2 g/L 0.8 g/L 2 GB/T 6682 HJ/T 91 HJ/T 164 HJ 442 3 4 GB/T 6682 4.1 CH3OH 4.2 C5H12O=2000 mg/L 4.3=20.0 mg/L 4.1 4.2 04 4.4 C6H5F=2000 mg/L 4.5=10.0 mg/L 4.1 4.4 04 4.6 99.999%4.7 99.999%DB46/T 4822019 2 5 5.1-/EI 5.2 5 ml 1/3 Tenax 1/3 1/3 5.3 60 m0.32 mm 1.8 m 6%/94%5.4 40 ml 5.5 10 l 25 l 50 l 250 l 5.6 6 6.1 HJ/T 91 HJ/T 164 HJ 422 5.4 6.2 4 14 15 d 7 7.1 7.1.1 5 ml 40 40 ml/min 11 min 180 2 min 180 10 min 7.1.2 45 2.0 min 10/min 120 20/min 200 1.0 min 200 2.0 ml/min 10:1 7.1.3 EI 70 eV 230 250 5.0 min/SIM 73 55 57 73 96 70 50 96 DB46/T 4822019 3 5.5 6.0 6.5 7.0 7.5 8.0 8.5 9.0 9.50.000.250.500.751.001.251.50 1 7.2 7.3 4.3 50 ml 1.0 g/L 5.0 g/L 10.0 g/L 20.0 g/L 50.0 g/L 5 ml 5.0 ml 5.0 l 4.5 7.1 2 1 1=10.0 g/L=10.0 g/L 7.3.1 i RRFi 1 i IsiISi iAARRFi 1 RRFi i Ai i AISi i ISi g/L i i g/L RRF 2 nRRFRRFnii 1 2 DB46/T 4822019 4 RRF RRFi i n RRF 3 1)(12-n=SDniiRRF RRF 3 RRF 4%100 RRFSD=RSD 4 RRF RSD 20%7.3.2 7.4 5.0 ml 5.0 l 4.5 10.0 g/L 7.1 7.3 3 4 7.5 7.4 8 8.1 3 30%8.2 8.2.1 x 5DB46/T 4822019 5 RRF Af A=ISIS xx 5 x g/L Ax IS g/L AIS RRF f 8.2.2 x 6 f=x 1 6 x g/L 1 g/L f 8.3 9 9.1 1.0 g/L 10.0 g/L 20.0 g/L 6 3.9%5.8%1.8%6.1%2.0%4.4%13.4%5.7%5.9%0.2 g/L 1.3 g/L 1.8 g/L 0.4 g/L 2.0 g/L 3.7 g/L 1.0 g/L 10.0 g/L 20.0 g/L 6 7.0 13.2%1.6 8.4%2.2 6.6%9.2%8.7%8.3%0.3 g/L 1.6 g/L 2.6 g/L 0.4 g/L 2.9 g/L 5.2 g/L 1.0 g/L 10.0 g/L 20.0 g/L 6 4.6 9.3%2.2 4.1%2.9 5.0%7.2%10.3%7.5%0.2 g/L 1.0 g/L 2.3 g/L 0.3 g/L 3.1 g/L 4.8 g/L 1.0 g/L 10.0 g/L 20.0 g/L 6 3.8 8.7%2.9 7.7%1.3 10.9%DB46/T 4822019 6 7.5%8.2%9.8%0.2 g/L 1.6 g/L 3.7 g/L 0.3 g/L 2.7 g/L 6.2 g/L 1.0 g/L 10.0 g/L 20.0 g/L 6 3.6 10.0%3.1 8.1%1.2 10.4%10.0%9.5%7.8%0.2 g/L 1.5 g/L 3.5 g/L 0.4 g/L 3.0 g/L 5.5 g/L 9.2 1.0 g/L 10.0 g/L 20.0 g/L 6 97%100%99%97%26%100%12%99%12%1.0 g/L 10.0 g/L 20.0 g/L 6 101%100%101%101%18%100%17%101%16%1.0 g/L 10.0 g/L 20.0 g/L 6 105%103%102%105%16%103%21%102%16%1.0 g/L 10.0 g/L 20.0 g/L 6 102%96%95%102%15%96%16%95%18%1.0 g/L 10.0 g/L 20.0 g/L 6 104%100%103%104%20%100%19%103%15%10 10.1 20 20/10.2 20%0.995 20 20/1 20%10.3 20 20/30%10.4 20 20/70%130%DB46/T 4822019 7 11 _
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